[warrensaged]

First,
If it rained in your evap dish, don't throw it out yet, but your probably out of luck on that one.
Second,
Start a new extraction. Defat this one!!! (take the time to do it, come on!!)
After you've basified the new bark solution, stir your naptha/water disapointment into it.
Re-check your pH to make sure you've not lowered it too much.
Continue on with your naptha pulls, etc... as normal.
...and freeze precipitate this time!!
Your probably gonna get a larger than normal yeild because you should actually be getting two yeilds!! (or at least close!)
If your wanting fluffy white crystals, you gotta do this as slow as it takes!! You can not rush a good thing!
Hope that helps!
WS