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| | #1 (permalink) |
| Mycophiliac Join Date: Aug 2007
Posts: 6
![]() | DMT Extraction Tek Hi everyone, I’ve been looking to extract some DMT for a while now, I’ve read numerous extraction teks and have decided to put one together based on what suits me best, can anyone see any problems with this: 1.Wash 500g MHRB in Naptha to remove any fats, filter with cheese cloth and discard Naptha. 2.Mix 2.5 litres water with 250g NaOH in 5 litre container, shake and let sit. 3.Add 500g MHRB to the solution, shake and let sit for an hour or so. 4.Add 250ml Naptha to solution, roll around on floor to agitate, DO NOT SHAKE, let sit and repeat 3 times and let sit for a while (1hr). 5.Once the layers have separated siphon off the Naptha and place to one side. 6.Wash Naptha once with Sodium Bicarbonate solution and twice with distilled water. 7.Then place in crystallising jar and put in freezer. 8.Repeat steps 4 to 6 three more times. Leave the 3rd extraction in the container for a couple of days, agitating occasionally to pick up any strays. 9.Leave jars in freezer for 24-72 hrs checking occasionally for forming DMT. 10.Pour each jar of Naptha through a coffee filter, save Naptha. Spread each filter out to dry thoroughly. 11.Pour 25ml of ICE COLD distilled water over coffee filter to wash out any contaminates, dry thoroughly again. Recrystallization 1.Place a small glass jar with the DMT and a small glass jar with Heptane together in a pan of hot water. 2.Little by little add 25ml of hot Heptane per gram of DMT, after a minute or two of heat the DMT should melt and mostly disappear into the solution. 3.Let it cool for a while to separate. 4.Carefully siphon as much of the clear Heptane as possible into a pyrex dish through filter paper. 5.Add another 5ml or so of Heptane to jar with sludge and heat again, then siphon as much clear Heptane off as possible in to the dish. 6.Repeat step 5 again. 7.Evaporate as slowly as possible 8.Scrape all the DMT into filter paper. 9.Pour 25ml of ICE COLD distilled water over the filter paper to clean even further, dry thoroughly. |
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| | #4 (permalink) | |
| Mycophage Join Date: Aug 2008
Posts: 142
![]() | Quote:
yes i didnt understand step one either.. that is a waste. also , yes you have to evaporate at least 1/2 of the naptha before you freeze precip. evaporate 1/2 to 2/3 , it will turn very cloudy and opaque.. THEN you put it in the freezer to freeze precip. wait like 18-36 hours.. dont 'check to see if dmt crystals are forming' as you say in your tek. It's ok to pick it up once to maybe look through the bottom and see the crystals (i know it's tempting), but dont open it up to look inside or you'll let moisture in. | |
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| | #5 (permalink) |
| Mycophage Join Date: Aug 2008
Posts: 142
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i have never recrystalized but im sure that will give you nice clean dmt. however i have never done this because i have never felt it necessary. once you have white freeze precip'd dmt, i just wash the dmt (once it is completely dried) , with cold non-sudsy ammonia . This leaves a clean, white, dmt powder that barely has a smell.. and is a pleasant smoke. never found it necessary to recrystalize, however it's probably cool to get clear dmt crystals, so do as you wish. |
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| | #7 (permalink) | ||||
| Mycotopiate Join Date: Oct 2006
Posts: 808
![]() ![]() ![]() ![]() ![]() ![]() ![]() ![]() ![]() ![]() ![]() | Quote:
that is not true, where are you getting your inforamtion arbol? there can be tons of crappy oils and shit that defats remove very effectivley. have you ever extracted DMT? no offense but i have never seen you post until a few days ago and every post i've seen has been not helpful and just pointless and irritating in general. whats with that? Quote:
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__________________ only those who risk going too far can find out how far one can go... | ||||
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| | #8 (permalink) |
| The Jester's Mad Chemist Join Date: Apr 2008
Posts: 1,258
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SWIM has done defats with MHRB and it was pointless...there were no oils. BUT, ive seen pictures of people doing defats that did pull out oils so i guess it depends on the bark. and also in that defat even tho its clear and theres no distinct oils it can still have stuff in there u cant see. I mean u dont see the oils in the np when u do the pulls but the in there.
__________________ Your trust is in Whiskey and Weed and Black Sabbath...its Goddamn Electric |
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